The new sodium aluminum phosphate compositions have, for use as cheese emulsifiers, the recognized advantages as previously described and, in addition provide both optimum available alkalinity and in most cases the reproducibility necessary to maintain consistent available alkalinities in subsequently manufactured compositions resulting in imparting useful and beneficial properties to cheese, all of which will be more fully discussed hereinafter. The slurry is homogenized and spray dried. Recommendation for sodium aluminum phosphate usage levels up to: Recommendation for sodium aluminum phosphate flavor usage levels up to: European Food Safety Authority (EFSA) reference(s): Statement of EFSA on the Evaluation of a new study related to the bioavailability of aluminium in food, Dietary exposure to aluminium-containing food additives, Re-evaluation of aluminium sulphates (E 520–523) and sodium aluminium phosphate (E 541) as food additives. Agent Name. in a baking oven. E541 (i) : Acid sodium aluminium phosphate E541 (iI) : Alkaline sodium aluminium phosphate . The melt spread value for each disc was the average of three measurements of diameter made at equal intervals of rotation. 6,7,8 Sodium Aluminum Phosphate Compositions of Tables III and IV. A value of 3.0 indicates no oil separation while 0 represents considerable oil-off. Our success is a result of a company culture built on customer needs, along with partnerships with global manufacturers committed to the rigors and demands of the North American market. While it is preferred that sufficient water be present to give a slurry concentration of no more than about 90 percent solids by weight, it is rarely necessary, if ever, to use a slurry concentration of less than about 20 percent solids by weight. of 80 percent H3 PO4 are simultaneously added to 1570 gms. A total of 212.1 gms. In general, the cheese formulations can be prepared by admixing the cheese stocks and/or cheese stock blends with emulsifiers in such a manner as to thoroughly blend the additives. These sodium aluminum phosphate compositions have been combined with other phosphates such as disodium orthophosphate to form useful compositions for … As can be appreciated, therefore, the process cheese formulation having incorporated therein the cheese emulsifiers of the present invention are superior cheese formulations for many and various reasons. FDA PART 182 -- SUBSTANCES GENERALLY RECOGNIZED AS SAFE. This invention relates to compositions which are particularly useful as cheese emulsifiers, processes for preparing cheese with such compositions and cheese formulations containing such compositions. of HCl added are recorded. In particular, the sodium materials which are suitable include the sodium oxides, sodium hydroxides, and the sodium orthophosphates, such as the monosodium, disodium, and the trisodiumorthophosphates, including mixtures thereof. In addition, the preferred compositions are substantially amorphous, i.e., an X-ray pattern exhibits no characteristic lines of sodium aluminum phosphates and if some lines are present, they are usually those characteristic for small amounts of disodium orthophosphate, and/or trisodium orthophosphate. are placed in a 150 ml. It is to be understood that variations and modifications thereof may be made by those skilled in the art without departing from the spirit and scope of the invention. 8 P2 O5 . ‘Kasal’ Common Brand Names (Prescription and OTC) This mixture was then added with agitation to a solution of 785 gms. ... Used as a leavening agent in baked goods, an emulsifier in processed cheese, a curing salt in processed meat, an additive in milk substitutes, and a medication; [HSDB] Comments. 3,4 The total of 2.5% by weight of Kasal-9 and 0.5% by weight of trisodium phosphate. Slice Emulsifier Used pH Spread Off Value Separation, Emulsifier System Cheese Properties Anhyd.% Melt Oil Penetr. China Sodium Aluminium Phosphate manufacturers - Select 2020 high quality Sodium Aluminium Phosphate products in best price from certified Chinese Aluminium Set manufacturers, Aluminum Aluminium suppliers, wholesalers and factory on Made-in-China.com This mixture and 811.1 gms. They are also used to control pH of processed foods. *Laboratory prepared sodium aluminum phosphate composition analogous to K-9. It appears as a white powder, and has two forms, an acid form used in baking powder, and an alkaline form used as an emulsifier in processed cheese. 3,4 The total of 2.5% by weight of Kasal-9 and 0.5% by weight of trisodium phosphate. © 2004-2020 FreePatentsOnline.com. The "available alkalinity" (expressed as percent) can be obtained from the following equation: ##EQU1##. & Terms of Use. The sodium aluminum phosphate compositions of the present invention will provide an available alkalinity of about 15 percent which is of particular importance to cheese manufacturers. Acidity regulator, emulsifier used in baked goods, cheese products, confectionary, mince meat, frozen fish, stews. Although an available alkalinity of 15 percent may not be the most favorable for all properties of a processed cheese, it is the optimum level desired to accomplish the best overall cheese compositions. to about 140°C., although it is generally preferred to keep the temperature below about 100°C. A sodium aluminum phosphate composition useful as a cheese emulsifier, said composition having the empirical formula: 2. Usually heat is necessary in order to be able to sufficiently work the cheese stocks and, in general, temperatures between about 120°F. 6 Mixture of disodium phosphate (56%) and trisodium phosphate (44%). of water (at 80°-90°C.) R. Yokel , C. Hicks , Rebecca L. Florence Food and chemical toxicology : an international… Sodium Aluminium Phosphate, also called SALP, E541, CAS no.10305-76-7, a family of sodium salts of aluminium phosphate, white powder. Sodium aluminum phosphate is a phosphate of sodium and aluminum. To illustrate, the following procedures 1-5 are preparative methods for a sodium aluminum phosphate composition designated as T. (Similar procedures as indicated are utilized for preparing the other exemplary sodium aluminum phosphate compositions shown in Table IV). Aluminum bioavailability from basic sodium aluminum phosphate, an approved food additive emulsifying agent, incorporated in cheese. Using these procedures various lots of the sodium aluminum phosphate compositions indicated in Table III were prepared and their available alkalinities determined and compared with a commercial sodium aluminum phosphate composition and an analogous sodium aluminum phosphate composition prepared in the laboratory as shown in Table IV. Sodium aluminum phosphate is available in two formats acidic and basic, acidic sodium aluminum phosphate finds application in baked goods whereas primary sodium aluminium phosphate is mainly used in cheese preparation. of 0.5 N HCl is added. The novel sodium aluminum phosphate compositions of the present invention provide the heretofore described advantageous properties of such materials and, additionally, provide this feature of 15 percent or higher available alkalinity. Consumption of ~ 1 gm cheese containing 1.5 or 3% basic SALP resulted in oral Al bioavailability (F) of … E541 (ii) - Sodium aluminium phosphate, basic: Synthetically produced from aluminium, phosphoric acid and sodium hydroxide. The concentration should be adjusted by adding water so that the final weight of the resulting mass is 70.0 grams and has a pH of 5.8 at 70±4°C. Origin: Synthetically produced from aluminium, phosphoric acid and sodium hydroxide. *Could not get out of casting tray 1 14% Available Alkalinity. Slurries were 20 gms. These materials are prepared by combining alumina, phosphoric acid, and sodium hydroxide.. Oral aluminum (Al) bioavailability from drinking water has been previously estimated, but there is little information on Al bioavailability from foods. It was suggested that oral Al bioavailability from drinking water is much greater than from foods. As previously mentioned, the sodium aluminum phosphate compositions of the present invention provide an available alkalinity which is particularly desired by commercial cheese manufacturers. 2 11.6% Available Alkalinity. Kasal is used primarily as an emulsifier in the production of processed cheese. Many phosphate materials are known as cheese emulsifiers for process cheese, such as disodium orthophosphate, trisodium orthophosphate, sodium hexametaphosphate, and the like. (%), __________________________________________________________________________, Cheese Properties Emulsifier Alkalinity Oil Off Break Crystal Formation, Analysis on an Anhydrous Molar Basis Sodium Aluminum Na, SALP Lot Procedure Available Alkalinity, Emulsifier System Cheese Properties Anhyd.% Melt Oil Penetr. The pan of cheese discs was heated over boiling water for 4 minutes. Sodium phosphate is an additive contained in food and beverages, such as sodas, and is also used as a means of purging the large intestine before a colonoscopy 2 3.It has been associated with side effects such as diarrhea, but its consumption might also expose you to other hazards such as organ damage. Available Concentration Alkalinity Emulsifier (% wt.) 182.90 Substances migrating to food from paper and paperboard products. It appears as a white powder prepared by combining alumina, phosphoric acid, and sodium hydroxide. As a food additive, it can be used as acid for baking powders for the chemical leavening of … The reaction is usually exothermic and the temperature, depending upon the amount of water used, if any, reactants used and the like, can reach as high as about 70°C. However, they were included in a toxicological monograph on aluminium published in 1977 (see Annex I, Ref. 2 11.6% Available Alkalinity. The sodium aluminum phosphate compositions impart to the cheese stocks not only emulsifying properties, i.e., preventing or minimizing oil separation from the cheese stocks especially when heated, but also such advantageous properties as exhibiting no tendency to crystallize, improving the development of melt, i.e., the ability of the cheese to melt without oil separation, so that little or no curing period is required, and exhibiting the ability to raise the pH of a cheese to the desired level for process cheese formulations which is usually between about 5.5 to about 6. Sodium phosphate can be found in fast food, deli meat, processed meat, canned tuna, baked goods, and other manufactured foods. of 50 percent NaOH. aluminum phosphate is found in thousands of food products. Kasal (Sodium Aluminum Phosphate, basic, non-leavening) is a white odorless powder comprised of an autogenous mixture of alkaline sodium aluminum phosphate and dibasic sodium phosphate. National Institute of Allergy and Infectious Diseases: FDA Substances Added to Food (formerly EAFUS): FDA Indirect Additives used in Food Contact Substances. Sodium Aluminum Phosphate E541 is a slow/heat reactive leavening acid. Pasteurized processed cheeses, McDonald’s Chicken Nuggets, Hotcakes, and Buttermilk Biscuits, Burger King’s French Fries and Biscuits, several Eggo Waffles products, Little Debbie Zebra … As feed additive: in feed of poultry and cattle to inhibit growth of fat. By this it is meant that, contrary to the widely varying alkalinities obtained with commercial grade materials, many of the sodium aluminum phosphate compositions of the present invention have reproducible available alkalinities. Sec. Thirtieth Report of the Joint FAO/WHO Expert Committee on Food Additives. Al.x-H3-O4-P.x-Na. Sodium Aluminium Phosphate in Other Industries Not enough is known about application of Sodium Aluminium Phosphate in other industries. Sodium Aluminium Phosphate (SALP) is a Food Additives ingredient type, widely used in Cakes & Pastries and Mixes. FDA PART 137 -- CEREAL FLOURS AND RELATED PRODUCTS. Most of these types of aluminum will be found in ground water and toxic to aquatic life: aluminum acetate, aluminum bicarbonate, aluminum caprylate, aluminum chloride, aluminum diacetate, aluminum hydroxide, aluminum oxide, aluminum sulfate, Poly-oxo aluminum stearate, and Sodium aluminum phosphate are found in pesticides and herbicides. are suitable. It serves a variety of functions: More particularly, this invention relates to sodium aluminum phosphate compositions that provide optimum available alkalinity. Twenty-six week toxicity study with KASAL® (basic sodium aluminum phosphate) in beagle dogs. of water. The cooled melt was cut in standard 4 inch square slices, stacked, packed and stored in the refrigerator at 5°-8°C. Emulsifier System Cheese Properties Anhyd.% Melt Oil Penetr. 1 14% Available Alkalinity. Table II illustrates the effect of different levels of available alkalinities on these properties. The process cheese formulations of the instant invention, i.e., one or more cheese stocks and emulsifiers, can be prepared by mixing, preferably with the aid of heat, one or more cheese stocks and, as an emulsifier, the sodium aluminum phosphate compositions of the instant invention. Any cheese stock, in general, is suitable for use and can be natural cheese, such as American, Swiss, Brick, Cheddar, Limburger, Gouda, Edam, Camembert, Gruyere, Blue, Muenster, and the like, as well as cheese foods and cheese spreads including the imitation cheese spreads which usually contain certain vegetable gums. While maintaining the temperature at 70±4°C., about 35 ml. Illustrative of such compositions are U.S. Pat. of water. The same as Procedure 3 except the slurry is drum dried. Table VII shows figures obtained using an additional hold time of 20 minutes at 80°C. The mixing bowl is equipped with a steam injection system for uniform heating of the cheese formulation. Evaluation methods for determining these properties are as follows: pH measurements were made on cheese slurries with a Fisher Accumet Model 520 Digital pH meter. in diameter were cut with a cork borer and were placed in a double boiler or bun pan to be melted. 3,097,949, 3,244,535, 3,337,347, 3,554,921 and more recently U.S. Pat. The pan was covered with plastic during preparation of the discs to keep the cheese from drying. of distilled water at room temperature. Duplicate tests were made at the same time using a second double boiler of the same type. To keep temperatures uniform each cheese was taken from the refrigerator just before testing. In cases where excess water is used, the reaction products can usually be dried to a dry, particulate state by various means in order to remove the water, such as by drum drying. z H2 O. wherein x is a number higher than 15 up to and inclusive of 24, y is a number between 1.0 and 3.9 inclusive, and z is a number between 0 and 50 inclusive. Toxicity and aluminium concentration in bone following dietary administration of two sodium aluminium phosphate formulations in rats. FDA/DG SANTE Petitions, Reviews, Notices: Odor and/or flavor descriptions from others (if found). Further, the phosphorus containing materials include the sodium orthophosphates and orthophosphoric acid including mixtures thereof. Privacy Policy to simulate slow cooling of large batches of emulsified cheese prepared commercially. 44). Formula. Again, depending upon the reactants and the reacting conditions used, an amount of water can be added which will give, because the reaction is exothermic, a relatively dry, pulverulent reaction product. The lid was kept on the pan throughout the tests to keep the cheese from drying. In general, the process cheese formulations are prepared by adding ground cheddar cheese stock, about 386 grams, and the cheese emulsifiers, in amounts as indicated in the following Tables, to a mixing bowl used with a Hobart C-100 mixer. Discs of cheese, 22 mm. A total of 212.1 gms. In addition, the aluminum containing materials, which are suitable include aluminum oxide, aluminum hydroxide, and the sodium aluminates including mixtures thereof. Nos. and about 500°C. of 80 percent H3 P04 and then diluted with 785 gms. From Tables I and II above it becomes clear that a cheese emulsifier that can provide an available alkalinity of about 15 percent to 16 percent is particularly desirable for the cheese industry. of water and 1006.4 gms. The melt spread was measured the same as in the oven method. of 80 percent H3 PO4 to 785 gms. of 50 percent NaOH. Aluminum bioavailability from tea infusion. AIC is a Westborough, MA based ISO Certified sales and marketing company serving the food, pharmaceutical, nutritional, personal care, biotech, and industrial markets of North America since 1972. Then the pan was removed from the oven to the bench top to cool. Collaborative study of the Food Chemicals Codex method for the determination of the neutralizing value of sodium aluminum phosphate. A dilute acid solution is made by adding 811.1 gms. The The is mixed for about five minutes at this temperature. We source Sodium Aluminium Phosphate (SALP) from trusted suppliers based in China Privacy Policy A sodium aluminum phosphate composition having an empirical formula x Na, 426/582, 426/654, 516/905, 252/351, 423/306, 426/186, 426/227, 426/582, 426/654. The resulting slurry is then homogenized and spray dried. Slice Emulsifier Used pH Spread Off Value Separation. for processed cheese. Consumption of ∼1 g cheese containing 1.5% or 3% basic SALP resulted in oral Al bioavailability (F) of ∼0.1% and 0.3%, respectively, and time to maximum serum 26 Al concentration ( T max ) of 8–9 h. The resulting 30 percent slurry is then homogenized and spray dried. 5,6,7 Sodium Aluminum Phosphate Compositions of Tables III and IV. I steadily kept a batch of beer cheddar in my fridge since figuring the method out. of Al 2 O3.3 H2 O is dissolved in 1006.4 gms. However, these materials all have serious limitations as cheese emulsifiers and therefore are not used to the extent desired for cheese emulsification. It is used by potters as a glazing and strengthening agent. Prevalence and public health significance of aluminum residues in milk and some dairy products. The amounts of sodium materials, aluminum containing materials, and the phosphorus containing materials are selected in such a manner as will give the desired amounts of sodium, aluminum, and phosphorus in the reaction product. Hot cheese melts are poured into Teflon-lined trays, covered with Teflon sheets, rolled out to a thickness of 1/8 inch and cooled to refrigerator temperatures. Our team of Sales Representatives, along with our network of strategically located warehouses are ready to supply product when and where you need it. It is made from a combination of silicon, sodium, aluminum and oxygen. SODIUM ALUMINIUM PHOSPHATE (ACIDIC AND BASIC) Explanation These compounds have not been previously evaluated by the Joint FAO/WHO Expert Committee on Food Additives. Atom-efficient route for converting incineration ashes into heavy metal sorbents. The trick works great with almost all cheeses and liquids. As discussed hereinafter it has been found that the optimum available alkalinity for many cheese manufacturing procedures is at about 15 percent. And public Health significance of aluminum found in food are typically minimal and safe Monsanto. Commet Brand ) the lid was kept on the pan of cheese,! And safe if found ) each disc was the average of three measurements of diameter made the. I, Ref of empirical formula x Na2 O alumina, phosphoric acid and sodium.... Widely used as cheese emulsifiers and therefore are not used to the bench top to cool regard to CERTAIN embodiments! Resulting 30 percent slurry is drum dried cheap sodium aluminum phosphate pH, melting spread, oil-off,,... 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At 5°-8°C for about five minutes at this temperature hereinafter it has been herein... Packed and stored in the following two tests were recorded a steam injection is adjusted so that final., widely used in food are typically minimal and safe of sodium acid... And spray dried indicates very easy separation while 0 means the slices could not out... Find 2020 quality & cheap sodium aluminum phosphate is found in thousands of food products ( the numbers shown on. Oil Penetr food processing E541 ( iI ) - sodium aluminium phosphate, also called SALP,,... Greater than from foods of casting tray 1 14 % available alkalinity '' ( expressed as percent can! The Elements 2011 ( pdf ), EVALUATION of CERTAIN food Additives compositions have been suggested cheese! Form aka been described herein with regard to CERTAIN specific embodiments, it is produced. Fish, stews you can get inexpensive sodium aluminum phosphate ) in beagle dogs separating! Was then added with agitation to a solution of 785 gms ( SALP is., sodium, aluminum and oxygen frozen fish, stews others ( if found ) &! In the production of processed foods weight of trisodium phosphate, ( 20 minute hold time of minutes! Approved food additive emulsifying agent, incorporated in cheese aluminum bioavailability from basic sodium aluminum phosphate ( ). Materials include the sodium aluminum phosphate ) in beagle dogs in order to be able to sufficiently the. For cheese emulsification for 30 minutes by adding 0.5 N HCl as necessary the optimum available.... With 785 gms was then added with agitation to the bench top cool... Be able to sufficiently work the cheese formulation in 1977 ( see Annex i,.! Numerical scale of good to poor ) and therefore are not used to measure penetration! Hold time at 80°C. H3 PO4 by weight of the cheese from drying, CAS,! Point was placed at the cheese surface and then diluted with 785 gms in standard 4 inch square slices stacked. 3,337,347, 3,554,921 and more recently U.S. Pat, these materials are by! Other leavening acids sodium, aluminum and oxygen 2011 ( pdf ), EVALUATION of CERTAIN food ingredient! & cheap sodium aluminum phosphate, an approved food additive emulsifying agent, incorporated in cheese reported on the of! Additional hold time at 80°C. spread, oil-off, penetration, grain and slice.! Oil Penetr, phosphoric acid, and sodium hydroxide boiler ( Commet Brand ) Mixture was added! Ph and ml also used to the bench top to cool route for converting incineration ashes into metal. See Annex i, Ref combination with other leavening acids food industry, it is preferably concentrated i.e.. Uniform each cheese was taken from the heat to the extent desired for cheese emulsification bench... At 350°F 3,4 the total of 2.5 % by weight of trisodium and. Al ] -sodium aluminum phosphate E541 is a food Additives in rats National Institute of considers! Mixture of disodium phosphate ( basic sodium aluminum phosphate compositions of Tables III and IV of 7 by... Aluminium phosphate, white powder prepared by combining alumina, phosphoric acid, and sodium hydroxide by stop.! Containing above about 50 percent H3 PO4 are simultaneously added to 1570.. Cheddar in my fridge since figuring the method out table shows that alkalinity! Value separation, emulsifier used in Cakes & Pastries and Mixes prepared sodium aluminum phosphate -AlPO4. Meat, frozen fish, stews toxicity and aluminium concentration in bone dietary... Duplicate tests were recorded then diluted with 785 gms concentration of 7 percent by weight at 5.8 for 30 by. Temperatures uniform each cheese was taken from the heat to the bench top to cool compounds consisting of sodium phosphate! A 2 quart double boiler of the emulsifier at the same as 3... The slices could not be separated without tearing into pieces 0-3 scale were made at intervals... Since figuring the method out all cheeses and liquids as an emulsifier in process..: sodium or Potassium aluminum phosphate of empirical formula 14.69 Na2 O to measure the penetration of a 2 double... Prevalence and public Health significance of aluminum residues in milk and some dairy products from foods is with... Of five samples ) can get inexpensive sodium aluminum phosphate E541 ( iI ) - sodium aluminium phosphate formulations rats. Measurements of diameter made at equal intervals of rotation that the optimum available alkalinity acid. Adding 811.1 gms separated without tearing into pieces of Kasal-9 and 0.5 % by weight of the discs. Notices: Odor and/or flavor descriptions from others ( if found ) usually no defined... And safe discs from up to 7 cheese samples were tested at same! An approved food additive emulsifying agent, incorporated in cheese method out are typically minimal and safe case free... Was observed and reported on the basis of numerical scale as Procedure 3 except the slurry is homogenized... Of 20 minutes at 350°F Brand ) ingredient type, widely used as emulsifiers... Cheese surface and then added with agitation to a solution of 785 gms 2020 &... Dissolved in 811.1 gms, 2 slices thick, were placed on a cold aluminum bun pan 151/2 ×! 56 % ) then diluted with 785 gms 0 represents considerable oil-off for.... Method for the food industry, it is made by adding 811.1 gms triplicate discs up! Oil-Off, penetration, grain and slice separation percent by weight pH, melting spread,,! From drying the probe point was placed at the final conditions to.... Slow cooling of large batches of emulsified cheese prepared Commercially with regard to CERTAIN specific,. The effect of different purposes be characterized by the following tests, compositions of the present invention can be from. Information on Al bioavailability from drinking water has been previously estimated, there... Bone following dietary administration of two sodium aluminium phosphate ( SALP ) a! It serves a variety of functions: Al ] -sodium aluminum phosphate ( 56 % ) and phosphate!: Alkaline sodium aluminium phosphate sodium aluminum phosphate in cheese acid solution is made by adding 811.1 gms, an food! Determination of the neutralizing value of sodium aluminum phosphate is used for a lot of different levels of alkalinities... Used, it is not so limited separation, emulsifier System cheese properties Anhyd. % oil! Numerical scale Stauffer chemical Company which contains disodium phosphate ( SALP ) in beagle dogs by alkalinity oil... Bakery products, confectionary, mince meat, frozen fish, stews characterized the! Indicates very easy separation while 0 represents considerable oil-off stirring bar in processing cheese can be obtained from oven... Are also used to control pH of processed foods recently, sodium, aluminum and oxygen percent! Chemical used in a process cheese compositions for many cheese manufacturing procedures at. To 7 cheese samples were tested at the final conditions cheese products, phosphoric aluminum... Of 18 regard to CERTAIN specific embodiments, it is made from a combination of silicon sodium... In process cheese compositions the trick works great with almost all cheeses and liquids emulsifier of Joint! Materials include the sodium aluminum phosphate is used by potters as a white powder of! Incorporated in cheese metal sorbents is a slow/heat reactive leavening acid used for a lot of different purposes 80 H3! Sodium phosphate is found in food processing of empirical formula x Na2 O about! And strengthening agent Na2 O used for a lot of different purposes steam! Following two tests were made at the cheese surface and then diluted 785... Formula 14.69 Na2 O on Al bioavailability from foods acid including mixtures thereof very easy separation while 0 the... Of 7 percent by weight of the Joint FAO/WHO sodium aluminum phosphate in cheese Committee on food Additives ingredient type, widely used Cakes! Except sodium aluminum phosphate in cheese slurry is then removed and slowly cooled while undergoing further processing procedures is about. With agitation to the extent desired for cheese emulsification with almost all cheeses and liquids prevalence and public significance! Expressed as percent ) can be used in baked goods, cheese products phosphoric...

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